Controllable conversion of cellulose nanocrystals to cellulose microspheres: Insight on the effect of parameters during spray drying, TAPPI Journal February 2025

 


Application: This paper focuses on the controlled preparation of cellulose microspheres. The morphology and structure of cellulose microspheres were regulated by controlling the size of CNCs, the concentration of CNCs, and the inlet temperature of spray drying, providing a wider application potential for cellulose.

TAPPI conference proceedings and presentations, technical papers, and publication articles provide technical and management data and solutions on topics covering the Pulp, Paper, Tissue, Corrugated Packaging, Flexible Packaging, Nanotechnology and Converting Industries.

Simply select the quantity, add to your cart and your conference paper, presentation or article will be available for immediate download.
Author: Qingjun Mengh, Wenliang Zheng, and Yang Xu
Controllable conversion of cellulose nanocrystals to cellulo
ABSTRACT: Cellulose microspheres, which have mainly been produced via the sol-gel method up until now, exhibit a promising potential for broad applications due to their regular microstructure and renewability. However, some issues with production of cellulose microspheres, such as the recycling of involved organic solvents and the removal of the residual solvents, should be solved. In this study, a cellulose nanocrystals (CNCs) suspension was used to produce cellulose microspheres via spray drying in order to avoid the use of organic solvents. The effects of CNCs particle size, CNCs concentration, and inlet temperature of spray drying on microstructure and particle size of cellulose microspheres were investigated. The results indicated that the optimal average particle size and concentration of CNCs used for obtaining cellulose microspheres were 106 nm and 0.1 wt%, respectively. Under the optimal conditions, cellulose microspheres with a regular spherical morphology and an average particle size of ca. 3 ìm were obtained. The sulfuric acid hydrolysis and spray drying process barely affected the crystalline structure of cellulose. However, the introduced sulfhydryl groups, which were confirmed by Fourier transform infrared spectroscopy results, degraded the thermostability of cellulose. Generally speaking, converting CNCs to cellulose microspheres via spray drying is beneficial for promoting the controllable and continuous production of cellulose microspheres.
0.00

New Releases

TAPPI PRESS Catalog eBook 2024


Experience the Power of Publications in the 2024 TAPPI Press Catalog


Open
 

Kraft Recovery Boilers, Third Edition  


Sponsored by the Recovery Boiler Program R&D Subcommittee of the American Forest & Paper Association (AF&PA) and published by TAPPI Press.


Purchase
 

Handbook For Pulp and Paper Technologists (The SMOOK Book), Fourth Edition

The best-selling text to introduce the entire technology of pulp and paper manufacture.

Purchase
 

Guidelines for Safe Assessment and Operation of Yankee Dryers  


A project of the Yankee Dryer Safety & Reliability Committee.

Purchase
 

Check our newest additions.


TAPPI Press offers some of the most in-depth resources and references for the forest products and related industries. 

See More
   
 

Available for Purchase – Conference Proceedings


TAPPI maintains a record of key conference papers, presentations, and other conference publications, available for purchase in a variety of formats.

See More